Fluid-actuated flow control valves

ABSTRACT

An apparatus is described for controlling a flow of a fluid therethrough while the apparatus is connected to a source of control fluid. The apparatus includes an input, a valve seat, a diaphragm, an output, and a diaphragm control space. The diaphragm control space is partially defined by the diaphragm, and includes a control fluid inlet and a control fluid outlet. The apparatus is operative to independently control a flow of control fluid into the diaphragm control space through the control fluid inlet and a flow of control fluid out of the diaphragm control space through the control fluid outlet. A deflection of the diaphragm in relation to the valve seat is responsive to a pressure of the control fluid in the diaphragm control space. The deflection of the diaphragm in relation to the valve seat is operative to control a fluidic flow resistance between the input and the output.

FIELD OF THE INVENTION

This invention relates to the field of fluid delivery and, morespecifically, to apparatus and methods for the flow-controlled deliveryof gases and liquids.

BACKGROUND OF THE INVENTION

Fluids (i.e., gases and liquids) are used in many manufacturingindustries. Within a manufacturing process, fluids are typicallydispensed with precision of flow rate, timing or both. Generally, fluiddispensing equipment has the ability to adjust the flow rate by means offlow control valves. A flow control valve regulates the opening of aflow path (i.e., an orifice) to suit the necessary flow rate.

In addition to the orifice, the flow rate also depends on the propertiesof the fluid, as well as its temperature and pressure. For a given fluidat steady temperature and pressure, stable flow rates may be determinedsimply by the setting of the flow control valve. However, in manypractical flow control systems, the combination of temperature andpressure instability, as well as the finite precision and accuracy ofthe flow control valve, may prohibit the attainment of adequately stableand/or repeatable flow rate. In addition, downstream from the flowcontrol valve, a plurality of valves, sensors and other elements mayalso impact flow rate stability. In such instances, a flow control valvemay incorporate a flow sensor and a tunable flow control valve to pursuethe desired flow rate. For that purpose, the flow control system drivesthe tunable flow control valve to adjust the actual flow rates, to beequal to the desired flow rate. This self-correcting fluid deliverymethod has been successfully adapted for automatic manufacturing in manydifferent industries.

Conventional flow control valves implement a variety of variable-orificedesigns. Commonly, the orifice is confined between two surfaces. One ofthe surfaces comprises a fluid flow inlet, commonly known as a “valveseat.” A second surface is mechanically actuated to vary the gap betweenthese surfaces and adjust the orifice. The second surface is oftenattached to a precision controlled mechanical actuator such as aprecision screw, a proportionally controlled solenoid or aproportionally controlled piezoelectric actuator. Typically, the impactof the gap on the flow rate is strongly nonlinear, especially for smallgaps. Given the nonlinearity, as well as limitations of mechanicalstability and precision, most manually driven, precision screw-basedvalves resort to designs that increase the surface area of the gap. Thisincreased area provides sufficient flow resistance at somewhat largergaps to reduce the impact of nonlinearity and the effects of mechanicalimperfections and screw backlash, thereby improving flow control.

One popular design, for example, implements a motion controlled taperedneedle and a matching cavity. This “needle valve” design enablesreasonably stable and repeatable manually controlled valves that arecapable of reliable flow control down to about 2% of the maximum flow,wherein maximum flow means the flow of a fully open valve. However,highest performing “metering needle valves” are prone to significantwear of the needle over the needle cavity. This wear is especiallypronounced when controlling the small gaps that provide flow rates lowerthan 5% of the maximum flow. Such wear results in both reduced valveperformance and the generation of particles. Particles that aregenerated in the flow control system and consequentially delivered intothe process via streams of fluids are detrimental to the quality of manyindustrial manufacturing applications and are therefore undesirable.Accordingly, needle valves are mainly implemented for applications thatdo not require frequent flow adjustment and are not very sensitive toparticulates. Moreover, they are best used when not pushed to controlflow rates below about 5% of their total range.

The precision of a manual flow control valve is adversely impacted bytemperature and pressure instabilities as well as potentiallyfluctuating impact of downstream components. Therefore, they havegrowingly become inadequate for precision manufacturing. Instead, flowcontrol valves (also known as Mass Flow control valves—MFCs) canactively and controllably adjust the orifice gap to yield desired flowrates regardless of mechanical precision and stability limitations.Likewise, they can correct for temperature and pressure fluctuations orthe impact of downstream components. They are also fully compatible withfactory automation and quality control systems, hence, their growingwidespread popularity. Within MFCs, flow control valves with gapcontrolling actuators adjust the orifice between a fixed plane and themoving end of the actuator, wherein a fluid entry port, commonly calleda “valve seat,” is defined on the fixed plane. Hence, the actuator isimmersed in the fluid with potential fluid contamination, actuatorcorrosion, jamming and particle generation. To address this issue, somedesigns provide a metallic diaphragm disposed between the actuator andthe valve seat, in compatibility with Ultra High Purity (UHP) standards.For example U.S. Pat. No. 8,162,286 to Sawada et al. and entitled“Piezoelectric Driven Control Valve” discloses a flow control valve witha piezoelectric actuator and a UHP design. Likewise, U.S. Pat. No.5,447,173 to Kazama et al. and entitled “Mass Flow Controller, OperatingMethod and Electromagnetic Valve” discloses a flow control valve with asolenoid actuator and UHP design.

FIG. 1 depicts a UHP-compliant flow control valve 100. A dome-shapedmetallic diaphragm 101 creates an all-metallic valve chamber 102 overvalve seat 103. Valve seat 103 is located substantially across from theconcave center of diaphragm 101. The orifice 104 is defined betweenvalve seat 103 and diaphragm 101. Within valve chamber 102, a fluidoutlet port 105 is also formed. Diaphragm 101 seals the fluid withinvalve chamber 102 to prevent fluid-actuator contact. The gap betweendiaphragm 101 and valve seat 103 is reduced when actuator 106 deformsdiaphragm 101 towards valve seat 103. Similarly, the gap is increasedwhen a retreat of actuator 106 allows diaphragm 101 to spring back awayfrom valve seat 103. Also indicated in FIG. 1 are flow sensor 107,controller 108, enclosure 109, inlet fitting 110 and outlet fitting 111.

Typically, conventional actuators are electrically driven in onedirection and mechanically returned in the other direction by a springin the case of solenoids, or by strain discharge in the case ofpiezoelectric actuators. Generally, well designed actuators can providenearly linear position change per electrical drive (current forsolenoids and voltage for piezoelectric actuators). As a result,linearly responding actuators may tune the orifice gap linearly.Nevertheless, linear gap tuning produces nonlinear flow change. Ideally,actuators should be able to correct a difference between actual flowrate and the desired (set point) flow rate instantaneously andaccurately. Likewise, they should also be able to respond to a set pointchange with speed and precision.

Automated flow control valves typically apply closed-loop,proportional-integral (PI) or proportional-integral-derivative (PID)algorithms to alter the gap and adjust the flow to match the set point.However, both PI or PID control algorithms, as well as other controlalgorithms known in the art, are not suitable for accurate andresponsive control of nonlinear systems. Particularly, nonlinearitymakes flow control parameters flow dependent. That means that, for agiven set of flow control parameters (i.e., particular PI or PIDconstants), controllers cannot accurately control the actual flow tomatch a set point beyond the single flow rate that was selected toinitially tune the system and extract the PI or PID constants. Usingthese same flow control parameters to control other flow rates oftenyields erroneous and sometimes oscillatory flow rates, as well assubstantially slower response. Likewise, erroneous and oscillatory flowrates may also be driven by temperature and inlet pressure change,drift, or other fluctuations. Similarly, many applications require themixing of several flow-controlled sources of different fluids. Somesystems also manipulate the mixing ratio during the process. Lastly,many mixing manifolds increase the pressure downstream from flow controlvalves. This increased downstream pressure acts to reduce the flow pergiven orifice, causing flow control valves to react to increase theorifice and match the actual flow to the set point. However, thatreaction repositions the entire flow dependent PI or PID parameters. Dueto nonlinearity, the shifts in the flow to gap dependence detunes thecontrol system into lower performance, which results in sluggishresponse, increased error and tendency for oscillations. To overcomethis problem, the flow control valves should ideally be tuned at themixing condition. This tuning has to be repeated iteratively to convergeall flow control valves into accurate and non-oscillatory control. Ifthe process requires mixing ratio changes, new control constants arepreferably deduced for all flow control valves and applied as part ofthe change. Even so, however, the mixing ratio is nevertheless undefinedand unstable during transitions between different settings.

These fundamental deficiencies may be partially addressed by invokingactuator and orifice designs with reduced nonlinearity and controllersthat apply microprocessors for flow versus actuator motion corrections(“gain scheduling”) as part of the closed-loop control. Likewise,implementing temperature compensation and integrating inlet pressurecontrol may tame the adverse impact of fluctuating or driftingtemperature and/or inlet pressure. In some cases, when controllingfluids with relatively high inlet pressures, a highly restrictive outletorifice may effectively suppress the destabilizing impact of downstreamcomponents and/or other flows in the system. It is also recognized thatflow control valves perform best when the size of the orifice isoptimized to the application given the flow range, the type of fluid,the temperature and the entire process system. Given these improvements,sophisticated modern flow control valves may operate adequately over arange of flow rates around 10-90% of maximum flow for a wide range ofapplications. At the same time, these modern flow control valves canmitigate the slow and oscillatory response at both the low and the high20-30% ends of the range, as well as erroneous transient performance atflow rates that are outside a very narrow range of the most optimizedflow rate. In addition, in order to cover a wider range, systems may usemultiple different flow control valves with different ranges. That said,range limitations still create the need for many different anddistinctive models of flow control valves, and thereby substantiallyincrease inventory size and cost for manufacturers.

Flow control valves are also applied to control the pressure withindelivery manifolds wherein the flow sensor is substituted for a pressuresensor and the flow control device is tasked with tuning the actualpressure to a set point pressure. These pressure controllers find usagein a variety of applications, such as fluid delivery into Atomic LayerDeposition (ALD) systems. In these particular applications, the pressurecontrollers allow pressure-controlled gas to be made available at theinlets of fluid delivery valves that drive the ALD processing. Suchfluid delivery valves for ALD are discussed in, for example, U.S. Pat.No. 7,744,060 to Sneh and entitled “Fail-safe Pneumatically ActuatedValve with Fast Time Response and Adjustable Conductance,” which ishereby incorporated by reference herein. When a fluid delivery valve isopened, precisely metered delivery is established with a flow rate thatis determined by the controlled inlet pressure and the conductance ofthe ALD valve. That delivery is shaped as a pulse. Accordingly, the flowcontrol valve of the pressure controller must accurately respond to thepulse by quick flow rate changes, essentially going between a zero flowrate when pressure is at the pressure set point and a flow ratesufficiently high to restore the pressure back to the set point duringand just after a pulse. The precision of this pressure control is vitalfor efficient usage of reactive gas, as well as to the implementation ofSynchronously Modulated Flow and Draw (SMFD) ALD, which is discussed inU.S. Pat. No. 6,911,092 to Sneh and entitled “ALD Apparatus and Method,”which is also hereby incorporated by reference herein. SMFD ALDimplements fast ALD processes with <500 millisecond (ms) cycle times andrecovery times between successive pulses trending to below 150 ms.Conventional pressure controllers struggle with such demandingapplications.

One other challenging application implements flow control valves aspressure controllers to control the pressure of inert gas that is usedto provide improved thermal contact to process heaters and improve theirisolation from process effluents. In particular, fragile heaters may bedisposed inside a heating chuck wherein heater to chuck contact and/orcomplete sealing of the heaters inside the chuck is not possible.Accordingly, helium gas (He) is applied to assist in heat transfer andprovide positive flow out of the chuck space to negate the penetrationof harsh process chemicals. Ideally, helium pressure inside the chuckshould be kept at the same value during idle, process and transitionsbetween idle and process so as to promote stable chuck temperature. Atypical sequence of idle, part-handling, idle, transition, process,transition challenges the pressure controller to adapt quickly to asequence of flow-1, no-flow, flow-1, transition to flow-2, flow-2,transition to flow-1, wherein flow-2 is smaller than flow-1 given theimpact of the process pressure. During part transfer, a shutoff valve istypically turned off, dropping the flow of helium to zero. It is theobjective of the flow control valves to quickly react to these varyingconditions so as to maintain the pressure at set value during the entirecycle while enduring the impact of significant flow rate changes.Conventional flow control valves struggle with this application.

In a similar application, inert gas is directed to prevent process fluidfrom reaching the backside of a wafer. In this application, inert gas isapplied into the gap between a chuck and the backside of the wafer. Afirst pressure sensor is applied to obtain the pressure in the processchamber. A second pressure sensor is applied to obtain the pressure atthe inert gas delivery line. In this case, the flow control valve istasked with controlling the pressure differential between the second andthe first pressure sensors to a given pressure differential set point,and to ensure that, independent of process pressure variability bydesign or due to imperfection, there is always a set point pressuredifferential to negate the flow of process chemicals into the gap. Heretoo, conventional flow control valves struggle with such a demandingapplication.

In some other common applications, precision controlled motion ofpneumatic or hydraulic actuators is used to propel parts handling,robotic motion, stamping, etc. In these applications, flow-controlledfluids (e.g., air or hydraulic fluids) determine the speed of thesemotions. Often the speed of robotic arms and parts handling has tofollow intricate and complex profiles with well-defined acceleration anddeceleration profiles. In addition, some of these motions have to beable to perform their tasks under different or time-variable loadconditions. To accommodate these requirements, flow control valves withadequate precision and fast response across wide ranges of flow ratesand with the ability to accommodate a wide range of loads are needed.Existing systems struggle with many of these applications, inparticular, when speed is of the essence.

Conventional flow control valves may also struggle to provide reliableoperation at high temperatures, to provide reliable low and zero flowperformance, and to provide mechanisms for fail safety, that is,mechanisms to automatically shut off when unexpected system conditionsare encountered. With few exceptions, conventional flow control valvesdo not provide UHP construction with proper resistance to fluidcontamination, valve corrosion, particle generation and jamming. Theseflow control valves with actuators immersed in the fluids are notsuitable to control the flow of most liquids. Most flow control valvescomprise a very small orifice as part of the means to be able to controlrelatively low flow rates from relatively high inlet pressures. Thesepermanent flow restrictors adversely slowed down the rate of purging anddecontaminating flow and pressure controllers and their manifolds priorto component replacement and/or the performance of maintenance.

In recent decades, many manufacturing processes have strived to improveefficiency, increase quality and reduce cost and waste. This trendgrowingly emphasizes reliable and precise automation as well as theability to use manufacturing equipment as much as possible over a widerange of different processes. Within that trend, flow and pressurecontrollers with improved speed and precision over a wide range of flowrate, inlet pressure and ambient conditions, are essential for optimal,low waste and repeatable processing.

For the foregoing reasons, there is a need for new designs for flowcontrol valves that address the above-identified deficiencies.

SUMMARY OF THE INVENTION

Embodiments in accordance with aspects of the invention provideapparatus and methods that address the above-identified needs.

Aspects of the invention are directed to an apparatus for controlling aflow of a fluid therethrough while the apparatus is connected to asource of control fluid. The apparatus comprises an input, a valve seat,a diaphragm, an output, and a diaphragm control space. The diaphragmcontrol space is partially defined by the diaphragm, and comprises acontrol fluid inlet and a control fluid outlet. The apparatus isoperative to independently control a flow of control fluid into thediaphragm control space through the control fluid inlet and a flow ofcontrol fluid out of the diaphragm control space through the controlfluid outlet. Moreover, a deflection of the diaphragm in relation to thevalve seat is responsive to a pressure of the control fluid in thediaphragm control space. Lastly, the deflection of the diaphragm inrelation to the valve seat is operative to control a fluidic flowresistance between the input and the output.

Additional aspects of the invention are directed to a method forcontrolling a flow of a fluid. The method comprises providing an input,a valve seat, a diaphragm, an output, and a diaphragm control space. Thediaphragm control space is partially defined by the diaphragm, andcomprises a control fluid inlet and a control fluid outlet. Moreover,the method further comprises the step of independently controlling aflow of control fluid into the diaphragm control space through thecontrol fluid inlet and a flow of control fluid out of the diaphragmcontrol space through the control fluid outlet. A deflection of thediaphragm in relation to the valve seat is responsive to a pressure ofthe control fluid in the diaphragm control space. Lastly, the deflectionof the diaphragm in relation to the valve seat is operative to control afluidic flow resistance between the input and the output.

The above-identified embodiments may provide several advantages. Moreparticularly, flow control valves in accordance with aspects of theinvention may, as just a few examples:

-   -   provide for both manual and automated flow and pressure control;    -   control both gas and liquid fluids;    -   perform reliably over wide ranges of flow, inlet pressure, and        temperature conditions;    -   provide, fast and accurate response to flow or pressure set        point changes, as well as fast and accurate response to changes        in process-driven downstream pressure, temperature and        inlet-pressure;    -   provide a failsafe response with true shutoff when undesired        system conditions are encountered;    -   not require permanent flow restrictors, allowing for quick and        efficient decontamination;    -   implement UHP construction, and thereby be suitable for        operation with a wide selection of fluids, including corrosive        and reactive fluids as well as liquids that contain dissolved        solids, colloidal solutions, oils and fuels;    -   operate such that they avoid particle generation; and    -   provide flow and pressure control over substantially the entire        range of flow and pressure control applications.

BRIEF DESCRIPTION OF THE DRAWINGS

These and other features, aspects, and advantages of the presentinvention will become better understood with regard to the followingdescription, appended claims, and accompanying drawings where:

FIG. 1 depicts a sectional view of a prior art flow control valve;

FIG. 2 shows a sectional view of a flow control valve in accordance witha first illustrative embodiment of the invention;

FIG. 3 shows a sectional view of the FIG. 2 flow control valve with itssolenoid valves depicted schematically;

FIG. 4 shows a sectional view of a flow control valve in accordance witha second illustrative embodiment of the invention;

FIG. 5 displays a graph of flow rate versus control fluid pressure for aprototype flow control valve similar to that shown in FIG. 4;

FIG. 6 shows a sectional view of a flow control valve in accordance witha third illustrative embodiment of the invention;

FIG. 7 shows a sectional view of a flow control valve in accordance witha fourth illustrative embodiment of the invention;

FIG. 8 shows a sectional view of a flow control valve in accordance witha fifth illustrative embodiment of the invention;

FIG. 9 shows a sectional view of a flow control valve in accordance witha sixth illustrative embodiment of the invention;

FIG. 10a shows a perspective view of a flow control valve including anintegrated high speed flow measurement sensor, in accordance with anillustrative embodiment of the invention; and

FIG. 10b shows a sectional view of the FIG. 10a flow control valve.

DETAILED DESCRIPTION OF THE INVENTION

While conventional flow and pressure control valves utilize mechanicalmeans for deflecting a diaphragm in relation to a valve seat to affectorifice geometry, aspects of the invention instead utilize the pressureof a control fluid on a diaphragm to produce a similar effect. FIG. 2shows a sectional view of a flow control valve 300 in accordance with afirst illustrative embodiment of the invention. The flow control valve300 comprises a metallic diaphragm 301 disposed so as to seal the flowpath between valve seat 303 and fluid outlet port 305. Orifice 304 isthereby formed between diaphragm 301 and valve seat 303. A sealeddiaphragm control space 302 is formed above diaphragm 301 and is partlydefined by the diaphragm 301. The diaphragm control space 302 comprisescontrol fluid inlet 323 and control fluid outlet 333. The flow controlvalve 300 also includes a flow or pressure sensor 307, inlet fitting310, outlet fitting 311, control fluid inlet 312, solenoid valve 320,solenoid valve 330, controller 308 and enclosure 309. Control fluid(e.g., compressed air) from control fluid inlet 312 is fed into solenoid320.

In operation, solenoids 320, 330 cooperate to modulate the pressure ofcontrol fluid inside the sealed diaphragm control space 302, and therebycontrol the amount of deflection of the diaphragm 301. Moreparticularly, when solenoid 320 is activated, normally-closed plunger321 pulls seal 322 upward to open a flow path through inlet 323 andraise the pressure inside diaphragm control space 302. This tends todeflect diaphragm 301 towards valve seat 303 and reduce orifice 304.Flow rate through the flow control valve 300 is thereby lowered.Conversely, when solenoid 330 is activated, normally-closed plunger 331pulls seal 332 upward to open a flow path through outlet 333 and lowerthe pressure inside diaphragm control space 302 by allowing controlfluid to flow out of vent port 335. Diaphragm 301 responds to thereduced pressure by deflecting away from valve seat 303 to increaseorifice 304 and increase the flow rate. Preferably, the diaphragm 304 isshaped to yield a nonlinear spring constant. This nonlinear response isdesigned to yield an advantageous relation between flow rate and thepressure of the control fluid in diaphragm control space 302. Forexample, in one or more non-limiting embodiments, the nonlinear responsemay produce a linear relation over a wide range of flow rates higherthan 200 standard cubic centimeters per minute (sccm), converging into aprogressively weakening dependence in the lower 0-200 sccm range.

FIG. 3 illustrates flow control valve 300 with solenoid valves 320, 330depicted with schematic symbols. Sensor reading cable 350, and solenoidactuation cables 351 and 352 are also illustrated schematically. Thecables 350, 351, 352 interface sensor 307 with controller 308, andcontroller 308 with solenoids 320, 330.

The flow control valve 300 may function to control flow rate orpressure. More particularly, flow control valve 300 is configured tocontrol flow rates when sensor 307 is acting as a flow sensor, whileflow control valve 300 is configured to control pressure when sensor 307is acting as a pressure sensor. The actual flow (or pressure) signal isread by controller 308 and compared with a set point value. The errorbetween reading and set point is then applied to adjust the pressure ofthe control fluid inside diaphragm control space 302 via solenoids 320,330. When the error is positive (set point exceeds the actual reading),solenoid 330 is actuated to decrease the control fluid pressure indiaphragm control space 302 and increase orifice 304. Conversely, whenthe error is negative, solenoid 320 is actuated to increase controlfluid pressure to reduce orifice 304. Once the flow rate (or pressure)is controlled to match the set point, the control fluid pressure isessentially latched inside diaphragm control space 302. Tests ofprototypes similar to the flow control valve 300 have shown that, atsteady inlet pressure and ambient temperature, the flow rate (orpressure) can be held steady under such latched conditions (i.e.,without actuation of the solenoids) at better than ±0.2% for severalhours. Accordingly, the flow control valve of the current invention isan “integrating system.” Therefore, the control algorithm does notrequire an integral term.

The controller 308 may comprise one or more microprocessors withassociated memory, which are collectively operative to signal thesolenoids 320, 330 at least in part in response to flow or pressuresignals received from flow or pressure sensor 307. In one or moreembodiments, the controller 308 may, for example, actuate solenoids 320,330 via a proportional-derivative (PD) determined duty cycle. Moreparticularly, the solenoids 320, 330 may be actuated at auser-selectable frequency with the fraction of “ON” versus “OFF” being afunction of the error via the PD parameters. In alternative embodiments,the controller 308 may actuate proportionally controlled solenoids 320,330 proportionally by a PD-determined current. The controller 308 mayapply the same PD parameters to the control of both solenoids 320, 330.However, in some cases, the controller 308 may also apply different PDparameters to controlling each solenoid 320, 330 for optimumperformance. Given the teachings herein, both P-based and PD-basedcontrol schemes, as well as other equally suitable control methods alsofalling within the scope of the invention, will already be familiar toone having ordinary skill in the relevant arts. Reference is also madeto J-P Corriou, Process Control: Theory and Applications, Springer 2004;and C. Smith, Practical Process Control: Tuning and Troubleshooting,John Wiley & Sons, 2009, which are both hereby incorporated by referenceherein.

FIG. 4 shows a sectional view of a flow control valve 500 in accordancewith a second illustrative embodiment of the invention. Flow controlvalve 500 differs from flow control valve 300 in that flow control valve500 comprises a failsafe metal sealed shutoff valve. In a manner similarto flow control valve 300, however, flow control valve 500 may be usedto control flow rates when sensor 507 is a flow sensor, or used tocontrol pressure when sensor 507 is a pressure sensor.

Within flow control valve 500, metallic diaphragm 501 is positioned suchthat it is operative to seal the flow path between valve seat 503 andfluid outlet port 505. Orifice 504 is formed between diaphragm 501 andvalve seat 503. A sealed diaphragm control space 502 is formed abovediaphragm 501. The diaphragm control space comprises control fluid inlet523 and control fluid outlet 533. The flow control valve 500 alsoincludes inlet fitting 510, outlet fitting 511, control fluid inlet 526,solenoid valve 520, solenoid valve 530, controller 508 and enclosure509. Fluid from inlet 526 (e.g., compressed air) is fed into solenoid520. When solenoid 520 is activated, plunger 521 opens a flow paththrough inlet 523 to raise the pressure inside diaphragm control space502 and deflect diaphragm 501 towards valve seat 503 to reduce orifice504. Flow rate is thereby reduced. Conversely, when solenoid 530 isactivated, normally closed plunger 531 opens a flow path through outlet533 and lowers the pressure inside diaphragm control space 502 byallowing control fluid to flow out of vent port 535. Diaphragm 501responds to the reduced pressure by deflecting away from valve seat 503to increase orifice 504 and increase the flow rate.

Flow control valve 500 comprises shutoff valve 550 to provide failsafeshutoff of diaphragm 501 via stem 552 when, for example, the pressure ofcontrol fluid is lost due to a system failure. Stem 552 can slide intocontrol space 502 via opening 557. At the same time, seal 558 maintainsthe overall fluid tightness of control space 502. Stem 552 is retainedto shutoff valve 550 by the force of spring 553, which is adapted tobias the stem 552 towards the diaphragm 501. The shutoff valve 550 isactuated open when pressurized control fluid (e.g., compressed air) isinjected into actuator space 559 so as to translate the piston 551against the spring 553 and away from the diaphragm 501. Piston 551 isequipped with sliding seal 554. Once shutoff valve 550 is actuated open,control fluid from actuator space 559 feeds into solenoid 520 via inlet526, where it is available to modulate the position of diaphragm 501.Preferably, in use, the retraction of stem 552 is adjusted to theminimum needed to allow diaphragm 501 a full range of motion by plunger556, as set by adjustment screw 555. That limited motion is desirablefor minimizing the acceleration of stem 552 when control fluid pressureis lost, and the consequent impact when stem 552 translates intodiaphragm 501 over valve seat 503. This impact is further reduced byrestricting the vent of air out of actuator space 559 when the airsupply at inlet 512 is deactivated. In actual reduction to practice,both measures were found to be very effective in preventing thegeneration of particles by the failsafe shutoff valve 550.

A prototype flow control valve similar in design to that shown in FIG. 4was utilized to determine the dependence of flow rate through theprototype flow control valve (labeled as “Flow” in sccm) on controlfluid pressure (labeled as “Pressure” in pounds per square inch absolute(PSIA)) inside the prototype flow control valve and pressing down on theprototype's diaphragm. FIG. 5 displays these dependencies at differentnitrogen gas inlet pressures, namely, 20, 30, 40, 200, 380, 760 and1,370 Torr. The data was taken at room temperature to control the flowof nitrogen gas using compressed air as the control fluid. It will benoted that all traces exhibit a region with a substantially lineardependence of flow on pressure at flows higher than about 200 sccm. Atlow inlet pressure (about 20-200 Torr), the traces eventually start tolevel off and converge into the maximum flow rate bound by the finiteconductance of the fully-open flow control valve and the test system (inthis particular case, between 800-1,000 sccm). This conductance is quitehigh for such low inlet pressures given that the prototype flow controlvalve does not include a permanent flow restriction. At higher inletpressures such as 380, 760 and 1,370 Torr, the linear region extendedfor the entire measurement, and the impact of conductance wasnegligible.

For most wide-range performance, PD parameters are preferably tunedwithin the linear part of flow rate versus control pressure, forexample, at higher than 200 sccm for inlet pressures higher than 300Torr in the example of FIG. 5. These parameters will not deteriorate theprecision in the flow rate range below 200 sccm since, in contrast toconventional flow control valves, flow rate dependence on the controlfluid pressure will moderate (i.e., become less sensitive to pressure).However, in that low flow range, the PD parameters derived in the linearrange will result in reduced response times, while, at the same time,maintaining the precision beyond that needed. Optionally, an improvementmay be made in that case with relatively simple “gain scheduling,” aswould be known to one having ordinary skill in the art. For example, thePD parameters may be extracted for several flow rates and used to fit asimple parameter versus flow rate formula. Then the actual flow ratewill be used to continuously deduce the PD parameters and relatedsolenoid duty cycle (or current).

The progressively weakening dependence at the 0-200 sccm rangeincreasingly improves the finesse at lower set points. This feature isexactly the opposite of conventional behavior, wherein the nonlinearitymeans progressively worsening finesse at lower set points. Beyond a fewhundred sccm (about 200 sccm in the example of FIG. 5), the lineardependence provides wide control range with more than adequate finesse.Moreover, if desired, the slope of both linear and weakening dependencesmay be easily controlled by the stiffness of the diaphragm through itsthickness, mechanical properties and shape. One or more alternativeembodiments may also utilize multiple diaphragms that are stackedbetween the flow-path and the diaphragm control space. Accordingly, flowcontrol valves in accordance with aspects of the invention are able tocontrol flow rates over 3-4 orders of magnitude and accommodate a5-3,000 Torr inlet pressure range with up to 200° C. continuousoperation temperature. Moreover, these flow control valves are easilypurged at high flow for quick and efficient decontamination of upstreamand downstream manifolds.

Above 300 Torr, the impact of the inlet pressure on the PD parametersmay also be compensated for by reducing the proportional constant byabout 40%. At the same time, the impact of ambient temperature up to200° C. was found to be negligible. In other words, the prototype flowcontrol valve was able to correct for inlet pressure and/or temperaturefluctuations. In applications wherein significant inlet pressurefluctuations, drifts or variability are expected, it is preferred toreduce the proportional constant by up to 35% to ensure that under worstcase conditions, the precision and stability of the flow rates are notcompromised. In some cases this modification will result in up to 35%slower response. Nevertheless, with the exception of few applicationsand systems wherein fast and substantial fluctuations of inletpressures, and/or fast and substantial variations in mixing ratios arecommon, the impact of the derivative constants are marginal and thealgorithm can be simplified to apply proportional control only.

As further presented in FIG. 5, at low inlet pressure, the flow rate maybe subjected to the limitations of fully open valve conductance.Accordingly, the impact of control fluid pressure slows downsubstantially in the high flow rate range. However, the prototype flowcontrol valve was still able to control the flow up to the highestpossible flow rate with precision. That is, applying the PD parametersfrom the linear portion of the flow versus control pressure dependenceresulted in precise control. However, response time slowed down with theincrease in flow rate. For example at 20 Torr inlet pressure, the pureresponse time of the prototype flow control valve was 20 ms after a setpoint increase by 200 sccm from 150 to 350 sccm, but required 80 ms fora set point increase by 200 sccm from 500 to 700 sccm. For mostapplications, this slower response time is still adequate and typicallyfaster than the response time of the sensor, the manifold, or theircombination.

U.S. Pat. No. 7,744,060 to Sneh and entitled “Fail-Safe PneumaticallyActuated Valve with Fast Time Response and Adjustable Conductance”(hereby incorporated by reference herein) describes a failsafenormally-closed (FSNC) pneumatic valve wherein a diaphragm is deflectedin response to the application of control fluid pressure thereon. Inthat valve, the timing of diaphragm deflection and the transport of airinto and out of a diaphragm control space above the diaphragm wastypically less that 0.1 ms. (See, e.g., FIG. 1d of the '060 Patent).This fast response time suggests that diaphragms like those discussedherein will respond practically instantaneously to changes in controlfluid pressure. Therefore, the response of the flow control valves inaccordance with embodiments of the invention is likely to be determinedby the speed and the conductance of the solenoids, as well as thesupply, controlling and vent pressures. Custom manufactured solenoidsmay have an ON/OFF response time of <0.5 ms. Moreover, the ON/OFFactuation time may be adjusted via gap controlling screws (like screws324 and 334 in FIG. 2), with higher speeds resulting in a conductancetradeoff. For example, 0.4 ms solenoid response times in the solenoidsof the prototype flow control valve corresponded to a flow of about 10standard liters per minute (sLm) therethrough with a 45 PSIA controlfluid inlet pressure feeding the solenoid. At that flow rate, a pressurechange of 5 PSIA within a ˜1 milliliter volume diaphragm control spacetakes about 2 ms. This pressure change will correspond, for example, toa flow rate change in the 200-2,500 sccm range for inlet pressures inthe 300-3,000 Torr range (FIG. 5). Off-the-shelf, high-speed solenoidvalves have response times in the of 1-3 ms range and support flow ratesof up to about 50 sLm at 45 PSIA. These characteristics result in a 5PSIA controlling pressure change in a diaphragm control space in therange of 1.5-4 ms. Proportional control, custom or off-the-shelfsolenoid valves can typically vary the flow at 45 PSIA in the range of0-5 sLm wherein a 5 PSIA change of pressure within a diaphragm controlspace can be as fast as 4 ms. These fundamentally fast response timesenable well-tuned PD control with 20-50 ms response time over a widerange of flow rates, inlet pressures and temperatures.

Response times of high quality flow sensors typically vary between 2-500ms. Response times of high quality pressure sensors typically varybetween 0.1-20 ms. In some cases, sensor response time is impacted byfluid residence time, which can vary in a wide range of 5-1,000 ms,depending on the manifold. Accordingly, in many cases, flow controlvalves in accordance with aspects of the invention will be the fastestcomponent, sometimes significantly. However, as part of the tuningprocess, the proportional algorithm constant may be made to slow downthe reaction of the flow control valve to account for slow sensorresponse and other potential delays in the system, and thereby allow thesensor sufficient time to “catch up” by the time the error is close tonil. Therefore, in most embodiments, it is preferable to determine thePD parameters for the flow control valves on the actual system ofinterest.

To accommodate substantially slow responding systems such as systemsthat control the flow of liquids into actuators, the response time ofthe solenoid valves may be adjusted down to better match the timescaleof the system, rather than for the purpose of speeding up solenoidswitching. For example, the response time of solenoid 320 may beextended when screw 324 is adjusted clockwise to limit the motion ofplunger 321 and reduce the flow of control fluid through inlet 323.Similarly, the response time of solenoid 330 may be extended when screw334 is adjusted clockwise to limit the motion of plunger 331 and reducethe flow of control fluid through outlet 333.

Flow control valves 300, 500, as well as other embodiments fallingwithin the scope of this invention, effectively prevent the generationof particles at the diaphragm/valve-seat area. This feature is due tothe extremely small impact of the diaphragm against the valve seat,given the diaphragm's small mass and its decelerating spring force.Likewise, the impact of the control fluid against the diaphragm isnegligible. Flow valves in accordance with aspects of the inventionthereby may set new standards for stable performance and lifetime.Multiple prototypes were, for example, tested to retain theirperformance after 1×10⁸ cycles at 20 Hertz (Hz) wherein, within eachcycle, the control fluid was cycled between 0-100 PSIA to exert themaximum deflection and retraction of the diaphragms.

A similar embodiment in accordance with aspects of the invention isdepicted in the sectional view in FIG. 6. As before, flow control valve500′ may be used to control flow rates when sensor 507 is a flow sensor,and used to control pressure when sensor 507 is a pressure sensor.Within the flow control valve 500′, a metallic diaphragm 501 is disposedto seal the flow path between polymer valve seat 503′ and fluid outletport 505. All other components and features are similar to flow controlvalve 500 in FIG. 4. A prototype flow control valve similar to the flowcontrol valve 500′ demonstrated a lower leak rate than a prototype witha metal valve seat. More particularly, the prototype with the polymervalve seat demonstrated a leak rate of <10⁻⁸ mBar×L/second with thevalve shut off (i.e., control fluid pressure at inlet 512 vented), whilethe prototype with the metal seat demonstrated a leak rate of about 10⁻⁶mBar×L/second. The leak rate in the flow control mode of the prototypewith the polymer seat, once the shutoff stem was actuated, was <5×10⁻⁹mBar×L/second when the control fluid pressure exceeded 70 PSIG.Nevertheless, ultimately, the choice for valve seat material may dependon the temperature range of operation. For example, PFA 450HP (“Teflon”;available from DuPont (Fayetteville, N.C., USA)) may be suitable for awide range of temperatures up to 200° C. Polychlorotrifluoroethene(“Kel-F”; available from Aetna Plastics (Valley View, Ohio, USA)) may besuitable for applications below 85° C.

Flow control valves in accordance with aspects of the invention may beparticularly well suited to the demands of ALD processing. Prototypeflow control valves (acting as pressure controllers) similar to the flowcontrol valve 500′ were applied to control the pressure within ALDdelivery manifolds. For that purpose, a 50-100 milliliter ALD supplytank was installed downstream from the flow control valves. Deliverypressure was typically controlled within the pressure range of 5-50 Torrwith delivery within the flow rate range of 100-5,000 sccm. Typically,the supply tank was sized to accommodate <10%, preferably <5%, of gasdraw during an ALD pulse. For example, a 75 milliliter tank was used fora 10 Torr controlled reactive gas that was pulsed for 10 ms at about 250sccm each cycle, resulting in <4.3% draw. With PD parameters tuned inthe linear range of >200 sccm flow rate and >300 Torr inlet pressure,response time of <25 ms was achieved for flow rates in the linearportion of the flow dependence on control fluid pressure. Applying thesePD parameters, response times of less than 100 ms were achieved for flowrates in the 0-200 sccm range, as well as for inlet pressures in the5-300 Torr range. Accordingly, flow control valves in accordance withaspects of the invention were demonstrated to accommodate the entirewide range of ALD delivery specifications, with one part number, andwithout gain scheduling. At the same time, the integrated shutoff valveprovided fail safety for interlocking the delivery of highly reactiveALD precursors against loss of power or control fluid pressure (in thiscase, air pressure), as well as multiple other potentially hazardoussituations.

Another illustrative embodiment depicted in FIG. 7 comprises a failsafepolymer seat flow control and shutoff valve 500″. However, instead ofutilizing a local pressure sensor in the manner of flow control valves500, 500′, flow control valve 500″ is instead configured to controlpressure in response to one or more remotely-installed pressure sensors.Flow control valve 500″ therefore includes sensor input connector 540,which may communicate with the remote pressure sensors via cables (notshown). Such remote sensing capabilities may be suitable forapplications such as controlling the pressure of an inert gas thatprotect fragile heaters disposed inside a heating chuck whereinheater-to-chuck contact and/or complete sealing of the heaters insidethe chuck are not possible. For that application, flow control valve500″ may quickly react to adjust to maintain the pressure at set valueindependent of time varying flow out of the chuck. Of course, inalternative embodiments, remotely-installed flow sensors may be utilizedin a similar manner to regulate downstream flow rates rather thanpressure.

In another exemplary application in accordance with aspects of theinvention, a manifold comprising two flow control valves 500″, tworemotely installed flow sensors (interfaced with the two flow controlvalves via their sensor input connectors 540), and two shutoff valvesprovides directional and speed control to a hydraulic actuator. Themanifold connects the first flow control valve 500″ and the secondshutoff valve to one side of the actuator, and connects the second flowcontrol valve 500″ and the first shutoff valve to the second side of theactuator. The hydraulic actuator can move in two opposite directions.Speed controlled motion in the first direction actuates the shutoffvalve of first flow control valve 500″ and provides a flow rate setpoint to the flow control valve. At the same time the first shutoffvalve is actuated open. As a result, flow controlled fluid is applied topropel the actuator with a well-defined speed while the fluid is drainedfrom the other side of the actuator via the first shutoff valve. Thespeed of the actuator is precisely related to the flow rate.Alternatively, flow control valves 500″ can directly control the linearspeed of the actuator when the flow sensors are substituted with linearspeed sensors. To stop the motion, the hydraulic actuator is “braked” bya simultaneous shutoff of both first flow control valve 500″ and firstshutoff valve, to halt the flow instantaneously. To move in the seconddirection, the shutoff valve of second flow control valve 500″ isactuated and a flow rate set point is provided to the flow controlvalve. At the same time the second shutoff valve is actuated open. As aresult, flow controlled fluid is applied to propel the actuator with awell-defined speed while the fluid is drained from the other side of theactuator via the second shutoff valve. In this particular application,the fast response and wide range of flow control valves 500″, as well asthe integrated shutoff valves, provide fast and accurate motion controlto hydraulic systems for improved processing, stamping, parts handling,robotic motion, and the like.

FIG. 8 shows a sectional view of a flow control valve 800 in accordancewith a fifth illustrative embodiment of the invention. In this flowcontrol valve 800, metallic diaphragm 801 is disposed to seal the flowpath between valve seat 803 and fluid outlet port 805. Orifice 804 isformed between diaphragm 801 and valve seat 803. A sealed diaphragmcontrol space 802 is formed above diaphragm 801. The diaphragm controlspace comprises control fluid inlet 823. The flow control valve 800 alsoincludes inlet fitting 810, outlet fitting 811, and control fluid inlet812.

In contrast to the several flow control valves discussed above, the flowcontrol valve 800 utilizes a pressure regulator 860 as opposed tosolenoids to regulate control fluid pressure in diaphragm control space802. In use, control fluid (e.g., compressed air) from inlet 812 is fedinto pressure regulator 860. Pressure regulator 860, in turn, ismanually adjusted via knob 861 to deliver control fluid at regulatedpressure past sensing diaphragm 862 and into diaphragm control space 802via flow path 823. The pressure regulated control fluid inserted intocontrol space 802 deflects the diaphragm 801 and thereby defines theorifice 804, which, for a stable temperature and inlet pressure,establishes the flow rate. Unlike conventional manual “needle valve”flow control valves, flow control valve 800 provides for a wide range offlow rate adjustment with improved sensitivity at low flow rates, nogeneration of particles, and long service life. In addition, unlikeconventional mechanical needle valves, flow control valve 800 can bereproducibly switched between a precise orifice and a fully open, highflow path by virtue of ON/OFF switching the control fluid at inlet 812.

A further improvement in accordance with aspects of the invention isfurther depicted in the sectional view in FIG. 9, which shows anillustrative manual flow control valve 900 comprising a failsafe shutoffvalve 950. In this particular, non-limiting embodiment, metallicdiaphragm 901 is disposed to seal the flow path between valve seat 903and fluid outlet port 905. Valve seat 903 comprises a polymer seal.Orifice 904 is formed between diaphragm 901 and seat 903. A sealeddiaphragm control space 902 is formed above diaphragm 901. Diaphragmcontrol space 902 comprises controlling fluid inlet 923. The flowcontrol valve 900 also includes inlet fitting 910, outlet fitting 911,control fluid inlet 912 and pressure regulator 960.

Flow control valve 900 comprises shutoff valve 950 to provide failsafeshutoff of diaphragm 901 via stem 952. Stem 952 can slide into controlspace 902 via opening 957 while seal 958 maintains the overall fluidtightness of diaphragm control space 902. Stem 952 is biased by theforce of spring 953 towards the diaphragm 901. The shutoff valve 950 isopened when pressurized control fluid (e.g., compressed air) is injectedinto actuator space 959 to actuate piston 951. Piston 951 is equippedwith sliding seal 954. Once shutoff valve 950 is actuated open, controlfluid (e.g., compressed air) from actuator space 959 feeds into pressureregulator 960 via inlet 926, where the control fluid is available forthe flow control valve 900. The retraction of stem 952 may be adjustedto the minimum needed to allow diaphragm 901 a full range of motion byplunger 956, as set by adjustment screw 955. That limited motion ispreferred for minimizing the acceleration of stem 952 and the consequentimpact when stem 952 impacts diaphragm 901 against valve seat 903. Thisimpact may be further reduced by restricting the vent of control fluidout of actuator space 959 when the control fluid supply at inlet 912 isdeactivated. In actual reduction to practice, both measures were foundvery effective in preventing the generation of particles by the shutoffmechanism.

The control fluid from inlet 926 is fed into pressure regulator 960.Pressure regulator 960 may be manually adjusted via knob 961 to delivercontrol fluid at regulated pressure into diaphragm control space 902 viaflow path 923. The pressure-regulated control fluid injected intodiaphragm control space 902 defines the orifice 904, which for a giventemperature and inlet pressure, defines the flow rate. Here again, incontrast to conventional manual “needle valve” flow control valves, flowcontrol valve 900 provides for a wide range of flow rate adjustment withimproved sensitivity at low flow rates, no generation of particles, andlong service life. With the added integrated failsafe shutoff valve 950,flow control valve 900 further provides a single component substitute tocommonly used two-component shutoff-valve/needle-valve combinations.

Flow control valves in accordance with embodiments of the invention mayalso be implemented with integrated high speed flow measurement sensors.FIGS. 10a and 10b show such a flow control valve 1000, with FIG. 10ashowing a perspective view of the flow control valve 1000 with asidewall removed and FIG. 10b showing a sectional view. The flow controlvalve 1000 shares many elements with the flow control valve 500′ in FIG.6, and these elements are labeled with like reference numerals. At thesame time, the flow control valve 1000 includes an integrated high speedflow measurement sensor comprising an upstream pressure sensor 507′, adownstream pressure sensor 507″, and an orifice 560. These additionalelements are located between the fluid outlet port 505 and the outletfitting 511. The orifice 560 is of a given size to provide a calibratedflow rate. The pressure sensors 507′, 507″ measure pressure on oppositesides of the orifice 560. More particularly, the upstream pressuresensor 507′ is operative to measure pressure at a first space in theflow control valve 1000, while the downstream pressures sensor 507″ isoperative to measure pressure at a second space. The second space is influidic communication with the first space through the orifice 560.

In a working prototype flow control valve matching that shown in FIGS.10a and 10b , the high speed flow measurement sensor was implementedwith two model 85-005A-0C pressure sensors from Measurement Specialties(Hampton Va., USA). These pressures sensors had <1 msec response times,and faithfully reflected the pulsed flow modulation during ALDprocessing. The prototype was utilized to precisely control the deliveryof precursors during ALD processing by maintaining the integrated valueof each pulse at set-point. For that purpose, the flow was integrated ata set interval, typically in the range of 2-5 msec, from zero-flow, tothe next zero flow. This feature enhanced the precision ofprecursor-delivery during the ALD processing that, in turn, improved theefficiency of the process. In addition, it enabled real time monitoringof downstream ALD valves and components.

The added ability to monitor downstream ALD valves and components is aresult of the fact that the pressure of the downstream pressure sensor507″ is related to the delivery of precursor, which is being controlledby that pressure, as well as by the conductance of the downstream ALDvalve and manifold. An increase of this pressure during processing maytherefore indicate that the conductance of the ALD valve is decliningdue to potential problems of malfunctioning, clogging, manifoldtemperature increase, etc. Likewise, a decrease of that pressure duringprocessing may indicate that the manifold temperature may be comingdown, or it could indicate that the ALD manifold has developed a leak.This ability to gain an early warning for potential malfunctions,enables, for the first time, real time monitoring of the performance ofan often complicated collection of pulsed valves with the ability to usethis monitoring for early detection of problems. Such early detection ofproblems is crucial for the ability to maintain production ALD equipmentat ultimate performance to ensure high yield manufacturing.

In closing, it should again be emphasized that the above-describedembodiments of the invention are intended to be illustrative only. Otherembodiments can use different types and arrangements of elements forimplementing the described functionality. These numerous alternativeembodiments within the scope of the invention will be apparent to oneskilled in the art.

All the features disclosed herein may be replaced by alternativefeatures serving the same, equivalent, or similar purposes, unlessexpressly stated otherwise. Thus, unless expressly stated otherwise,each feature disclosed is one example only of a generic series ofequivalent or similar features.

What is claimed is:
 1. An apparatus for controlling a flow of anapparatus-controlled fluid therethrough while the apparatus is connectedto a source of diaphragm control fluid, the apparatus comprising: aninput; a valve seat; a diaphragm; an output; and a diaphragm controlspace, the diaphragm control space partially defined by the diaphragmand comprising a diaphragm control fluid inlet and a diaphragm controlfluid outlet; wherein the apparatus is operative to independentlycontrol a flow of diaphragm control fluid into the diaphragm controlspace through the diaphragm control fluid inlet and a flow of diaphragmcontrol fluid out of the diaphragm control space through the diaphragmcontrol fluid outlet; wherein a deflection of the diaphragm in relationto the valve seat is responsive to a pressure of diaphragm control fluidin the diaphragm control space; wherein the deflection of the diaphragmin relation to the valve seat is operative to control a fluidic flowresistance between the input and the output; wherein the diaphragmcontrol fluid is independent of the apparatus-controlled fluid.
 2. Theapparatus of claim 1, further comprising a diaphragm control fluid feedvalve, the diaphragm control fluid feed valve operative to regulate theflow of diaphragm control fluid into the diaphragm control space.
 3. Theapparatus of claim 2, further comprising a stem, the stem operative toslide towards and away from the diaphragm; a spring, the spring applyinga spring bias force against the stem towards the diaphragm; and a stemcontrol space, the stem control space operative to receive diaphragmcontrol fluid from the source of diaphragm control fluid; wherein apressure of diaphragm control fluid in the stem control space urges thestem in a direction opposite to the spring bias force.
 4. The apparatusof claim 3, wherein the stem control space is in serial fluidiccommunication with the diaphragm control fluid feed valve, and thediaphragm control fluid feed valve is in serial fluidic communicationwith the diaphragm control space.
 5. The apparatus of claim 3, whereinthe stem passes through a wall of the diaphragm control space.
 6. Theapparatus of claim 2, wherein the diaphragm control fluid feed valvecomprises a pressure regulator.
 7. The apparatus of claim 2, furthercomprising a diaphragm control fluid relief valve, the diaphragm controlfluid relief valve operative to regulate the flow of diaphragm controlfluid out of the diaphragm control space.
 8. The apparatus of claim 7,wherein the diaphragm control fluid feed valve comprises a solenoidvalve.
 9. The apparatus of claim 7, wherein the diaphragm control fluidrelief valve comprises a solenoid valve.
 10. The apparatus of claim 7,further comprising a controller, the controller operative to actuate thediaphragm control fluid feed valve and the diaphragm control fluidrelief valve.
 11. The apparatus of claim 10, further comprising asensor, the sensor in data communication with the controller.
 12. Theapparatus of claim 11, wherein the sensor is operative to measure atleast one of flow and pressure.
 13. The apparatus of claim 11, whereinthe controller is operative to actuate the diaphragm control fluid feedvalve and the diaphragm control fluid relief valve at least in partbased on data received from the sensor.
 14. The apparatus of claim 13,wherein the controller is operative to actuate the diaphragm controlfluid feed valve and the diaphragm control fluid relief valve at leastin part based on data received from the sensor so as to achieve a sensorset point on the sensor.
 15. The apparatus of claim 10, wherein thecontroller is operative to actuate the diaphragm control fluid feedvalve and the diaphragm control fluid relief valve at least in partbased on data received from a sensor, the sensor being distinct from theapparatus and being operative to measure at least one of flow andpressure.
 16. The apparatus of claim 1, wherein the valve seat comprisesa metal or a polymer.
 17. The apparatus of claim 1, wherein thediaphragm control fluid comprises a gas or a liquid.
 18. The apparatusof claim 1, further comprising: an upstream pressure sensor, theupstream pressure sensor operative to measure pressure at a first spacein the apparatus; a downstream pressure sensor, the downstream pressuressensor operative to measure pressure at a second space in the apparatus;and an orifice; wherein the second space is in fluidic communicationwith the first space through the orifice.
 19. A method of controlling aflow of an apparatus-controlled fluid comprising the steps of: providingan input: providing a valve seat; providing a diaphragm; providing anoutput; providing a diaphragm control space, the diaphragm control spacepartially defined by the diaphragm and comprising a diaphragm controlfluid inlet and a diaphragm control fluid outlet; and independentlycontrolling a flow of diaphragm control fluid into the diaphragm controlspace through the diaphragm control fluid inlet and a flow of diaphragmcontrol fluid out of the diaphragm control space through the diaphragmcontrol fluid outlet; wherein a deflection of the diaphragm in relationto the valve seat is responsive to a pressure of diaphragm control fluidin the diaphragm control space; wherein the deflection of the diaphragmin relation to the valve seat is operative to control a fluidic flowresistance between the input and the output wherein the diaphragmcontrol fluid is independent of the apparatus-controlled fluid.